[ { "instruction": "\n You are an expert at extracting quantity, units and their related context from text. \n Given a paragraph below identify each quantity and its related unit and related context, i.e. the measured entity and measured property if they exist.\n ", "paragraph": "30. The method of claim 27, wherein the precursor material has an average particle size (D50) in the range from 7-13 microns.", "measurement_extractions": [ { "docId": "CA2806915A1_30", "quantity": "in the range from 7-13 microns", "unit": "microns", "measured_entity": "the precursor material", "measured_property": "average particle size (D50" } ], "split": "train", "docId": "CA2806915A1_30", "dataset": "bm" }, { "instruction": "\n You are an expert at extracting quantity, units and their related context from text. \n Given a paragraph below identify each quantity and its related unit and related context, i.e. the measured entity and measured property if they exist.\n ", "paragraph": "31. The method of claim 16, wherein the precursor material has a tap density in the range from 0.8-2.8 g/cm3.", "measurement_extractions": [ { "docId": "CA2806915A1_31", "quantity": "in the range from 0.8-2.8 g/cm3", "unit": "g/cm3", "measured_entity": "the precursor material", "measured_property": "tap density" } ], "split": "train", "docId": "CA2806915A1_31", "dataset": "bm" }, { "instruction": "\n You are an expert at extracting quantity, units and their related context from text. \n Given a paragraph below identify each quantity and its related unit and related context, i.e. the measured entity and measured property if they exist.\n ", "paragraph": "33. The method of claim 16, wherein the precursor material has a surface area in the range from 2-20 m2/g.", "measurement_extractions": [ { "docId": "CA2806915A1_33", "quantity": "in the range from 2-20 m2/g", "unit": "m2/g", "measured_entity": "the precursor material", "measured_property": "surface area" } ], "split": "train", "docId": "CA2806915A1_33", "dataset": "bm" }, { "instruction": "\n You are an expert at extracting quantity, units and their related context from text. \n Given a paragraph below identify each quantity and its related unit and related context, i.e. the measured entity and measured property if they exist.\n ", "paragraph": "9. The precursor material of claim 1, wherein the precursor material has a tap density in the range from 0.8-2.8 g/cm3.", "measurement_extractions": [ { "docId": "CA2806915A1_9", "quantity": "in the range from 0.8-2.8 g/cm3", "unit": "g/cm3", "measured_entity": "the precursor", "measured_property": "tap density" } ], "split": "train", "docId": "CA2806915A1_9", "dataset": "bm" }, { "instruction": "\n You are an expert at extracting quantity, units and their related context from text. \n Given a paragraph below identify each quantity and its related unit and related context, i.e. the measured entity and measured property if they exist.\n ", "paragraph": "10. Precursor material according to claim 9, wherein the precursor material has a tap density of 1.8-2.3 g/cm3range.", "measurement_extractions": [ { "docId": "CN103108833A_10", "quantity": "1.8-2.3 g/cm3", "unit": "g/cm3", "measured_entity": "precursor", "measured_property": "tap density" } ], "split": "train", "docId": "CN103108833A_10", "dataset": "bm" }, { "instruction": "\n You are an expert at extracting quantity, units and their related context from text. \n Given a paragraph below identify each quantity and its related unit and related context, i.e. the measured entity and measured property if they exist.\n ", "paragraph": "11. Precursor material according to claim 1, wherein the precursor material in the surface area of 2-20m2/g range.", "measurement_extractions": [ { "docId": "CN103108833A_11", "quantity": "2-20m2/g", "unit": "m2/g", "measured_entity": "precursor", "measured_property": "surface area" } ], "split": "train", "docId": "CN103108833A_11", "dataset": "bm" }, { "instruction": "\n You are an expert at extracting quantity, units and their related context from text. \n Given a paragraph below identify each quantity and its related unit and related context, i.e. the measured entity and measured property if they exist.\n ", "paragraph": "12. Precursor material according to claim 11, wherein the precursor material in the surface area of 2-8m2/g range.", "measurement_extractions": [ { "docId": "CN103108833A_12", "quantity": "2-8m2/g", "unit": "m2/g", "measured_entity": "precursor", "measured_property": "surface area" } ], "split": "train", "docId": "CN103108833A_12", "dataset": "bm" }, { "instruction": "\n You are an expert at extracting quantity, units and their related context from text. \n Given a paragraph below identify each quantity and its related unit and related context, i.e. the measured entity and measured property if they exist.\n ", "paragraph": "13. Precursor material according to claim 1, wherein the precursor materials within the sodium level is less than 500 ppm.", "measurement_extractions": [ { "docId": "CN103108833A_13", "quantity": "500 ppm", "unit": null, "measured_entity": "precursor", "measured_property": "sodium level" } ], "split": "train", "docId": "CN103108833A_13", "dataset": "bm" }, { "instruction": "\n You are an expert at extracting quantity, units and their related context from text. \n Given a paragraph below identify each quantity and its related unit and related context, i.e. the measured entity and measured property if they exist.\n ", "paragraph": "14. Precursor material according to claim 13, wherein the precursor materials within the sodium level is less than 300 ppm.", "measurement_extractions": [ { "docId": "CN103108833A_14", "quantity": "300 ppm", "unit": "ppm", "measured_entity": "precursor", "measured_property": "sodium level" } ], "split": "train", "docId": "CN103108833A_14", "dataset": "bm" }, { "instruction": "\n You are an expert at extracting quantity, units and their related context from text. \n Given a paragraph below identify each quantity and its related unit and related context, i.e. the measured entity and measured property if they exist.\n ", "paragraph": "21. Method according to claim 16, wherein the alkaline hydroxide pH of the solution was maintained at about 11-13 within a range.", "measurement_extractions": [ { "docId": "CN103108833A_21", "quantity": "about 11-13 within a range", "unit": null, "measured_entity": "pH", "measured_property": null } ], "split": "train", "docId": "CN103108833A_21", "dataset": "bm" }, { "instruction": "\n You are an expert at extracting quantity, units and their related context from text. \n Given a paragraph below identify each quantity and its related unit and related context, i.e. the measured entity and measured property if they exist.\n ", "paragraph": "28. Method according to claim 16, wherein in the reactor at about 50-70 \u00b0C performed at a temperature in the range of co-precipitation.", "measurement_extractions": [ { "docId": "CN103108833A_28", "quantity": "50-70 \u00b0C", "unit": "\u00b0C", "measured_entity": "in the reactor", "measured_property": "temperature" } ], "split": "train", "docId": "CN103108833A_28", "dataset": "bm" }, { "instruction": "\n You are an expert at extracting quantity, units and their related context from text. \n Given a paragraph below identify each quantity and its related unit and related context, i.e. the measured entity and measured property if they exist.\n ", "paragraph": "29. Method according to claim 16, wherein the precursor material has an average particle diameter (D50) in the 3-30 microns.", "measurement_extractions": [ { "docId": "CN103108833A_29", "quantity": "3-30 microns", "unit": "microns", "measured_entity": "precursor", "measured_property": "average particle diameter (D50" } ], "split": "train", "docId": "CN103108833A_29", "dataset": "bm" }, { "instruction": "\n You are an expert at extracting quantity, units and their related context from text. \n Given a paragraph below identify each quantity and its related unit and related context, i.e. the measured entity and measured property if they exist.\n ", "paragraph": "30. Method according to claim 27, wherein the precursor material has an average particle diameter (D50) at 7-13 microns.", "measurement_extractions": [ { "docId": "CN103108833A_30", "quantity": "7-13 microns", "unit": "microns", "measured_entity": "precursor", "measured_property": "average particle diameter (D50" } ], "split": "train", "docId": "CN103108833A_30", "dataset": "bm" }, { "instruction": "\n You are an expert at extracting quantity, units and their related context from text. \n Given a paragraph below identify each quantity and its related unit and related context, i.e. the measured entity and measured property if they exist.\n ", "paragraph": "31. Method according to claim 16, wherein the precursor material has a tap density is 0.8-2.8 g/cm3range.", "measurement_extractions": [ { "docId": "CN103108833A_31", "quantity": "0.8-2.8 g/cm3", "unit": "g/cm3", "measured_entity": "precursor", "measured_property": "tap density" } ], "split": "train", "docId": "CN103108833A_31", "dataset": "bm" }, { "instruction": "\n You are an expert at extracting quantity, units and their related context from text. \n Given a paragraph below identify each quantity and its related unit and related context, i.e. the measured entity and measured property if they exist.\n ", "paragraph": "32. Method according to claim 31, wherein the precursor material has a tap density of 1.8-2.3 g/cm3range.", "measurement_extractions": [ { "docId": "CN103108833A_32", "quantity": "1.8-2.3 g/cm3", "unit": "g/cm3", "measured_entity": "precursor", "measured_property": "tap density" } ], "split": "train", "docId": "CN103108833A_32", "dataset": "bm" }, { "instruction": "\n You are an expert at extracting quantity, units and their related context from text. \n Given a paragraph below identify each quantity and its related unit and related context, i.e. the measured entity and measured property if they exist.\n ", "paragraph": "33. Method according to claim 16, wherein the precursor material in the surface area of 2-20m2/g range.", "measurement_extractions": [ { "docId": "CN103108833A_33", "quantity": "2-20m2/g", "unit": "m2/g", "measured_entity": "precursor", "measured_property": "surface area" } ], "split": "train", "docId": "CN103108833A_33", "dataset": "bm" }, { "instruction": "\n You are an expert at extracting quantity, units and their related context from text. \n Given a paragraph below identify each quantity and its related unit and related context, i.e. the measured entity and measured property if they exist.\n ", "paragraph": "34. Method according to claim 33, wherein the precursor material in the surface area of 2-8m2/g range.", "measurement_extractions": [ { "docId": "CN103108833A_34", "quantity": "2-8m2/g", "unit": "m2/g", "measured_entity": "precursor", "measured_property": "surface area" } ], "split": "train", "docId": "CN103108833A_34", "dataset": "bm" }, { "instruction": "\n You are an expert at extracting quantity, units and their related context from text. \n Given a paragraph below identify each quantity and its related unit and related context, i.e. the measured entity and measured property if they exist.\n ", "paragraph": "35. Method according to claim 16, wherein the precursor materials within the sodium level is less than 500 ppm.", "measurement_extractions": [ { "docId": "CN103108833A_35", "quantity": "less than 500 ppm", "unit": "ppm", "measured_entity": "precursor", "measured_property": "sodium level" } ], "split": "train", "docId": "CN103108833A_35", "dataset": "bm" }, { "instruction": "\n You are an expert at extracting quantity, units and their related context from text. \n Given a paragraph below identify each quantity and its related unit and related context, i.e. the measured entity and measured property if they exist.\n ", "paragraph": "36. Method according to claim 35, wherein the precursor materials within the sodium level is less than 300 ppm.", "measurement_extractions": [ { "docId": "CN103108833A_36", "quantity": "less than 300 ppm", "unit": "ppm", "measured_entity": "precursor", "measured_property": "sodium level" } ], "split": "train", "docId": "CN103108833A_36", "dataset": "bm" }, { "instruction": "\n You are an expert at extracting quantity, units and their related context from text. \n Given a paragraph below identify each quantity and its related unit and related context, i.e. the measured entity and measured property if they exist.\n ", "paragraph": "7. Precursor material according to claim 1, wherein the precursor material has an average particle diameter (D50) in the 3-30 microns.", "measurement_extractions": [ { "docId": "CN103108833A_7", "quantity": "3-30 microns", "unit": "microns", "measured_entity": "precursor", "measured_property": "average particle diameter (D50" } ], "split": "train", "docId": "CN103108833A_7", "dataset": "bm" }, { "instruction": "\n You are an expert at extracting quantity, units and their related context from text. \n Given a paragraph below identify each quantity and its related unit and related context, i.e. the measured entity and measured property if they exist.\n ", "paragraph": "8. Precursor material according to claim 7, wherein the precursor material has an average particle diameter (D50) at 7-13 microns.", "measurement_extractions": [ { "docId": "CN103108833A_8", "quantity": "7-13 microns", "unit": "microns", "measured_entity": "precursor", "measured_property": "average particle diameter (D50" } ], "split": "train", "docId": "CN103108833A_8", "dataset": "bm" }, { "instruction": "\n You are an expert at extracting quantity, units and their related context from text. \n Given a paragraph below identify each quantity and its related unit and related context, i.e. the measured entity and measured property if they exist.\n ", "paragraph": "9. Precursor material according to claim 1, wherein the precursor material has a tap density is 0.8-2.8 g/cm3range.", "measurement_extractions": [ { "docId": "CN103108833A_9", "quantity": "0.8-2.8 g/cm3", "unit": "g/cm3", "measured_entity": "precursor", "measured_property": "tap density" } ], "split": "train", "docId": "CN103108833A_9", "dataset": "bm" }, { "instruction": "\n You are an expert at extracting quantity, units and their related context from text. \n Given a paragraph below identify each quantity and its related unit and related context, i.e. the measured entity and measured property if they exist.\n ", "paragraph": "4. 1 according to claim-any one of claims 3 Li-Ni composite oxide particles, characterized in:\nAn average particle diameter 1-20 \u00b5m, a specific surface area BET 0.1-1.6 m2/g.", "measurement_extractions": [ { "docId": "CN104704659A_4", "quantity": "1-20 \u00b5m", "unit": "\u00b5m", "measured_entity": "Li-Ni composite oxide particles", "measured_property": "average particle diameter" }, { "docId": "CN104704659A_4", "quantity": "0.1-1.6 m2/g", "unit": "m2/g", "measured_entity": "Li-Ni composite oxide particles", "measured_property": "specific surface area BET" } ], "split": "train", "docId": "CN104704659A_4", "dataset": "bm" }, { "instruction": "\n You are an expert at extracting quantity, units and their related context from text. \n Given a paragraph below identify each quantity and its related unit and related context, i.e. the measured entity and measured property if they exist.\n ", "paragraph": "5. Claim 1-4 of, any one Li-Ni producing composite oxide particles, characterized in:\nWith powder of a lithium compound Ni-Co hydroxide particles mixed powder, firing the obtained mixture,\nNi-Co hydroxide particles obtained by powder, aqueous solution comprising a metal sulfate, aqueous ammonia and aqueous sodium hydroxide mixed, controls such that the reaction tank ammonia concentration is 1.4 mol/L or less, and the (ammonia concentration of the reaction vessel)/(concentration of remaining reaction tank hvdroxide) of 6 or more, obtaining Ni-Co hydroxide.", "measurement_extractions": [ { "docId": "CN104704659A_5", "quantity": "1.4 mol/L", "unit": "mol/L", "measured_entity": "controls such that the reaction tank", "measured_property": "ammonia concentration" } ], "split": "train", "docId": "CN104704659A_5", "dataset": "bm" }, { "instruction": "\n You are an expert at extracting quantity, units and their related context from text. \n Given a paragraph below identify each quantity and its related unit and related context, i.e. the measured entity and measured property if they exist.\n ", "paragraph": "6. Claim 1-4 of, any one Li-Ni producing composite oxide particles, characterized in:\nA powder of a lithium compound, Ni-Co hydroxide particle powder, aluminum powder and/or zirconium compound mixing powder of the compound, firing the obtained mixture,\nNi-Co hydroxide particles obtained by powder, aqueous solution comprising a metal sulfate, aqueous ammonia and aqueous sodium hydroxide mixture, ammonia concentration is 1.4 mol/L so that the reaction tank is controlled below, and the (ammonia concentration of the reaction vessel)/(concentration of the reaction vessel remaining hvdroxide) of 6 or more, obtaining Ni-Co hydroxide.", "measurement_extractions": [ { "docId": "CN104704659A_6", "quantity": "1.4 mol/L", "unit": "mol/L", "measured_entity": "reaction tank", "measured_property": "ammonia concentration" } ], "split": "train", "docId": "CN104704659A_6", "dataset": "bm" }, { "instruction": "\n You are an expert at extracting quantity, units and their related context from text. \n Given a paragraph below identify each quantity and its related unit and related context, i.e. the measured entity and measured property if they exist.\n ", "paragraph": "8. The lithium transition metal oxide according to claim 1, wherein the average particle diameter D50 of the transition metal precursor is 1 \u03bcm to 30 \u03bcm.", "measurement_extractions": [ { "docId": "CN104884390B_8", "quantity": "1 \u03bcm to 30 \u03bcm", "unit": "\u03bcm", "measured_entity": "transition metal precursor", "measured_property": "average particle diameter D50" } ], "split": "train", "docId": "CN104884390B_8", "dataset": "bm" }, { "instruction": "\n You are an expert at extracting quantity, units and their related context from text. \n Given a paragraph below identify each quantity and its related unit and related context, i.e. the measured entity and measured property if they exist.\n ", "paragraph": "1. A method for producing transition metal composite hydroxide particles serving as a precursor of a positive electrode active material for a nonaqueous electrolyte secondary battery by a crystallization reaction, comprising:\na nucleus-forming step of controlling an aqueous solution for nucleus formation containing at least a transition metal-containing metal compound and an ammonium ion donor so that the aqueous solution for nucleus formation has a pH of 12.0 to 14.0 at a liquid temperature of 25 \u2103 and forming nuclei,\na particle growth step of controlling the aqueous solution for particle growth containing the nuclei obtained in the nucleus production step so that the pH of the aqueous solution for particle growth becomes lower than that in the nucleus production step at a liquid temperature of 25 \u2103 and 10.5 to 12.0 to grow the nuclei,\nthe reaction environment in the initial stage of the nucleus generation step and the particle growth step is a non-oxidizing environment having an oxygen concentration of 5 vol% or less, and the reaction environment is switched from the non-oxidizing environment to an oxidizing environment having an oxygen concentration of more than 5 vol% and then from the oxidizing environment to a non-oxidizing environment having an oxygen concentration of 5 vol% or less by performing environmental control at least once in the particle growth step.", "measurement_extractions": [ { "docId": "CN105122517A_1", "quantity": "12.0 to 14.0", "unit": null, "measured_entity": "aqueous solution for nucleus formation", "measured_property": "pH" }, { "docId": "CN105122517A_1", "quantity": "25 \u2103", "unit": "\u2103", "measured_entity": "aqueous solution for nucleus formation", "measured_property": "liquid temperature" }, { "docId": "CN105122517A_1", "quantity": "25 \u2103", "unit": null, "measured_entity": "particle growth", "measured_property": "liquid temperature" }, { "docId": "CN105122517A_1", "quantity": "10.5 to 12.0", "unit": null, "measured_entity": "particle growth", "measured_property": "pH" } ], "split": "train", "docId": "CN105122517A_1", "dataset": "bm" }, { "instruction": "\n You are an expert at extracting quantity, units and their related context from text. \n Given a paragraph below identify each quantity and its related unit and related context, i.e. the measured entity and measured property if they exist.\n ", "paragraph": "16. A positive electrode active material for nonaqueous electrolyte secondary battery, wherein,\nthe positive electrode active material for a nonaqueous electrolyte secondary battery is composed of secondary particles formed by aggregating a plurality of primary particles,\nthe secondary particles have a central portion of a hollow structure or a hollow structure, and have at least a space portion where the primary particles are not present and a shell portion electrically connected to the central portion outside the central portion,\nthe secondary particles have an average particle diameter of 1 to 15 [ mu ] m, and the [ (d90-d 10)/average particle diameter ] as an index indicating the width of the particle size distribution is 0.7 or less.", "measurement_extractions": [ { "docId": "CN105122517A_16", "quantity": "1 to 15 [ mu", "unit": "mu", "measured_entity": "the secondary particles", "measured_property": "average particle diameter" }, { "docId": "CN105122517A_16", "quantity": "0.7 or less", "unit": null, "measured_entity": "the secondary particles", "measured_property": "the particle size distribution" } ], "split": "train", "docId": "CN105122517A_16", "dataset": "bm" }, { "instruction": "\n You are an expert at extracting quantity, units and their related context from text. \n Given a paragraph below identify each quantity and its related unit and related context, i.e. the measured entity and measured property if they exist.\n ", "paragraph": "19. The positive electrode active material for a nonaqueous electrolyte secondary battery according to any one of claims 16 to 18, wherein the specific surface area is 0.7m2/g\uff5e3.0m2/g\u3002", "measurement_extractions": [ { "docId": "CN105122517A_19", "quantity": "0.7m2/g\uff5e3.0m2/g", "unit": "m2/g", "measured_entity": "positive electrode active material", "measured_property": "specific surface area" } ], "split": "train", "docId": "CN105122517A_19", "dataset": "bm" }, { "instruction": "\n You are an expert at extracting quantity, units and their related context from text. \n Given a paragraph below identify each quantity and its related unit and related context, i.e. the measured entity and measured property if they exist.\n ", "paragraph": "7. Transition metal composite hydroxide particles which are precursors of positive electrode active materials for nonaqueous electrolyte secondary batteries, wherein,\nthe transition metal composite hydroxide particles are composed of a plurality of plate-like primary particles and secondary particles formed by aggregating fine primary particles smaller than the plate-like primary particles,\nthe secondary particles have a central portion formed by the aggregation of the plate-like primary particles, and have at least one layered structure formed by the lamination of a low-density portion formed by the aggregation of the fine primary particles and a high-density portion formed by the aggregation of the plate-like primary particles outside the central portion,\nthe secondary particles have an average particle diameter of 1 to 15 [ mu ] m, and the [ (d90-d 10)/average particle diameter ] as an index indicating the width of the particle size distribution is 0.65 or less.", "measurement_extractions": [ { "docId": "CN105122517A_7", "quantity": "1 to 15 [ mu", "unit": "mu", "measured_entity": "the secondary particles", "measured_property": "average particle diameter" }, { "docId": "CN105122517A_7", "quantity": "0.65 or less", "unit": null, "measured_entity": "the secondary particles", "measured_property": "particle size distribution" } ], "split": "train", "docId": "CN105122517A_7", "dataset": "bm" }, { "instruction": "\n You are an expert at extracting quantity, units and their related context from text. \n Given a paragraph below identify each quantity and its related unit and related context, i.e. the measured entity and measured property if they exist.\n ", "paragraph": "1. Transition metal composite hydroxide particles which are precursors of positive electrode active materials for nonaqueous electrolyte secondary batteries, wherein,\nthe transition metal composite hydroxide particles are composed of a plurality of plate-like primary particles and secondary particles formed by aggregating fine primary particles smaller than the plate-like primary particles,\nthe secondary particles have a central portion formed by the aggregation of the plate-like primary particles, and have a layered structure formed by the lamination of a low-density portion formed by the aggregation of the fine primary particles and a high-density portion formed by the aggregation of the plate-like primary particles outside the central portion,\nthe average value of the ratio of the outer diameter of the central portion to the particle diameter of the secondary particles is 30 to 80%, and the average value of the ratio of the thickness of the high-density portion in the diameter direction to the particle diameter of the secondary particles is 5 to 25%,\nthe secondary particles have an average particle diameter of 1 to 15 [ mu ] m, and the [ (d90-d 10)/average particle diameter ] as an index indicating the width of the particle size distribution is 0.65 or less.", "measurement_extractions": [ { "docId": "CN105122517B_1", "quantity": "1 to 15 [ mu", "unit": "mu", "measured_entity": "the secondary particles", "measured_property": "average particle diameter" }, { "docId": "CN105122517B_1", "quantity": "0.65 or less", "unit": null, "measured_entity": "the secondary particles", "measured_property": "particle size distribution" } ], "split": "train", "docId": "CN105122517B_1", "dataset": "bm" }, { "instruction": "\n You are an expert at extracting quantity, units and their related context from text. \n Given a paragraph below identify each quantity and its related unit and related context, i.e. the measured entity and measured property if they exist.\n ", "paragraph": "11. A method for producing transition metal composite hydroxide particles serving as a precursor of a positive electrode active material for a nonaqueous electrolyte secondary battery by a crystallization reaction, the method comprising:\na nucleus-forming step of controlling an aqueous solution for nucleus formation containing at least a transition metal-containing metal compound and an ammonium ion donor so that the aqueous solution for nucleus formation has a pH of 12.0 to 14.0 at a liquid temperature of 25 \u2103 and forming nuclei,\na particle growth step of controlling the aqueous solution for particle growth containing the nuclei obtained in the nucleus production step so that the pH of the aqueous solution for particle growth becomes lower than that in the nucleus production step at a liquid temperature of 25 \u2103 and 10.5 to 12.0 to grow the nuclei,\nand the reaction environment at the initial stage of the nucleus generation step and the particle growth step is a non-oxidizing environment having an oxygen concentration of 5% by volume or less,\nin the particle growth step, the environmental control is performed 2 or more times, and the environmental control is performed by: the reaction environment is switched from the non-oxidizing environment to an oxidizing environment in which the oxygen concentration exceeds 5% by volume, and then from the oxidizing environment to a non-oxidizing environment in which the oxygen concentration is 5% by volume or less,\nthe total crystal reaction time in the oxidizing environment in the particle growth step is 3% to 30% of the total time in the particle growth step, and the crystal reaction time in each oxidizing environment is 1% or more of the total time in the particle growth step.", "measurement_extractions": [ { "docId": "CN105122517B_11", "quantity": "12.0 to 14.0", "unit": null, "measured_entity": "aqueous solution for nucleus formation", "measured_property": "pH" }, { "docId": "CN105122517B_11", "quantity": "25 \u2103", "unit": "\u2103", "measured_entity": "aqueous solution for nucleus formation", "measured_property": "liquid temperature" }, { "docId": "CN105122517B_11", "quantity": "25 \u2103", "unit": "\u2103", "measured_entity": "the aqueous solution for particle growth", "measured_property": "liquid temperature" }, { "docId": "CN105122517B_11", "quantity": "10.5 to 12.0", "unit": null, "measured_entity": "the aqueous solution for particle growth", "measured_property": "pH" } ], "split": "train", "docId": "CN105122517B_11", "dataset": "bm" }, { "instruction": "\n You are an expert at extracting quantity, units and their related context from text. \n Given a paragraph below identify each quantity and its related unit and related context, i.e. the measured entity and measured property if they exist.\n ", "paragraph": "19. A positive electrode active material for a nonaqueous electrolyte secondary battery, which is represented by the general formula (B): li1+uNixMnyCozMtO2The positive electrode active material is composed of lithium transition metal composite oxide particles having a hexagonal crystal structure and a layered structure, and in the general formula (B), -0.05. ltoreq. u.ltoreq.0.50, x + y + z + t 1, 0.3. ltoreq. x.ltoreq.0.95, 0.05. ltoreq. y.ltoreq.0.55, 0. ltoreq. z.ltoreq.0.4, 0. ltoreq. t.ltoreq.0.1, M is one or more additive elements selected from Mg, Ca, Al, Ti, V, Cr, Zr, Nb, Mo, Hf, Ta, W,\nthe positive electrode active material for a nonaqueous electrolyte secondary battery is composed of secondary particles formed by aggregating a plurality of primary particles,\nthe secondary particles have a central portion having a hollow structure or a hollow structure, and a space portion having no primary particles and an outer shell portion electrically connected to the central portion outside the central portion,\nand the average value of the ratio of the outer diameter of the central portion to the particle diameter of the secondary particles is 30 to 80%, the average value of the ratio of the thickness of the outer shell portion in the diameter direction to the particle diameter of the secondary particles is 5 to 25%,\nthe secondary particles have an average particle diameter of 1 to 15 [ mu ] m, and the [ (d90-d 10)/average particle diameter ] as an index indicating the width of the particle size distribution is 0.7 or less.", "measurement_extractions": [ { "docId": "CN105122517B_19", "quantity": "1 to 15 [ mu", "unit": "mu", "measured_entity": "secondary particles", "measured_property": "average particle diameter" }, { "docId": "CN105122517B_19", "quantity": "0.7 or less", "unit": null, "measured_entity": "secondary particles", "measured_property": "particle size distribution" } ], "split": "train", "docId": "CN105122517B_19", "dataset": "bm" }, { "instruction": "\n You are an expert at extracting quantity, units and their related context from text. \n Given a paragraph below identify each quantity and its related unit and related context, i.e. the measured entity and measured property if they exist.\n ", "paragraph": "20. The positive electrode active material for a nonaqueous electrolyte secondary battery according to claim 19, wherein the specific surface area is 0.7m2/g\uff5e3.0m2/g\u3002", "measurement_extractions": [ { "docId": "CN105122517B_20", "quantity": "0.7m2/g\uff5e3.0m2/g", "unit": "m2/g", "measured_entity": "positive electrode active material", "measured_property": "specific surface area" } ], "split": "train", "docId": "CN105122517B_20", "dataset": "bm" }, { "instruction": "\n You are an expert at extracting quantity, units and their related context from text. \n Given a paragraph below identify each quantity and its related unit and related context, i.e. the measured entity and measured property if they exist.\n ", "paragraph": "21. A positive electrode active material for a nonaqueous electrolyte secondary battery, which is represented by the general formula (B): li1+uNixMnyCozMtO2The positive electrode active material is composed of lithium transition metal composite oxide particles having a hexagonal crystal structure and a layered structure, and in the general formula (B), -0.05. ltoreq. u.ltoreq.0.50, x + y + z + t 1, 0.3. ltoreq. x.ltoreq.0.95, 0.05. ltoreq. y.ltoreq.0.55, 0. ltoreq. z.ltoreq.0.4, 0. ltoreq. t.ltoreq.0.1, M is one or more additive elements selected from Mg, Ca, Al, Ti, V, Cr, Zr, Nb, Mo, Hf, Ta, W,\nthe positive electrode active material for a nonaqueous electrolyte secondary battery is composed of secondary particles formed by aggregating a plurality of primary particles,\nthe secondary particles have a central portion of a hollow structure or a hollow structure, and have at least a space portion where the primary particles are not present and an outer shell portion electrically connected to the central portion outside the central portion, and at least one inner shell portion between the space portion and the outer shell portion,\nthe secondary particles have an average particle diameter of 1 to 15 [ mu ] m, and the [ (d90-d 10)/average particle diameter ] as an index indicating the width of the particle size distribution is 0.7 or less.", "measurement_extractions": [ { "docId": "CN105122517B_21", "quantity": "1 to 15 [ mu", "unit": "mu", "measured_entity": "the secondary particles", "measured_property": "average particle diameter" }, { "docId": "CN105122517B_21", "quantity": "0.7 or less", "unit": null, "measured_entity": "the secondary particles", "measured_property": "particle size distribution" } ], "split": "train", "docId": "CN105122517B_21", "dataset": "bm" }, { "instruction": "\n You are an expert at extracting quantity, units and their related context from text. \n Given a paragraph below identify each quantity and its related unit and related context, i.e. the measured entity and measured property if they exist.\n ", "paragraph": "23. The positive electrode active material for a nonaqueous electrolyte secondary battery according to claim 21 or 22, wherein the specific surface area is 0.7m2/g\uff5e3.0m2/g\u3002", "measurement_extractions": [ { "docId": "CN105122517B_23", "quantity": "0.7m2/g\uff5e3.0m2/g", "unit": "m2/g", "measured_entity": "positive electrode active material", "measured_property": "specific surface area" } ], "split": "train", "docId": "CN105122517B_23", "dataset": "bm" }, { "instruction": "\n You are an expert at extracting quantity, units and their related context from text. \n Given a paragraph below identify each quantity and its related unit and related context, i.e. the measured entity and measured property if they exist.\n ", "paragraph": "4. Transition metal composite hydroxide particles which are precursors of positive electrode active materials for nonaqueous electrolyte secondary batteries, wherein,\nthe transition metal composite hydroxide particles are composed of a plurality of plate-like primary particles and secondary particles formed by aggregating fine primary particles smaller than the plate-like primary particles,\nthe secondary particles have a central portion formed by the aggregation of the plate-like primary particles, and have a laminated structure in which a low-density portion formed by the aggregation of the fine primary particles and a high-density portion formed by the aggregation of the plate-like primary particles are laminated outside the central portion,\nthe secondary particles have an average particle diameter of 1 to 15 [ mu ] m, and the [ (d90-d 10)/average particle diameter ] as an index indicating the width of the particle size distribution is 0.65 or less.", "measurement_extractions": [ { "docId": "CN105122517B_4", "quantity": "1 to 15 [ mu", "unit": "mu", "measured_entity": "the secondary particles", "measured_property": "average particle diameter" }, { "docId": "CN105122517B_4", "quantity": "0.65 or less", "unit": null, "measured_entity": "the secondary particles", "measured_property": "particle size distribution" } ], "split": "train", "docId": "CN105122517B_4", "dataset": "bm" }, { "instruction": "\n You are an expert at extracting quantity, units and their related context from text. \n Given a paragraph below identify each quantity and its related unit and related context, i.e. the measured entity and measured property if they exist.\n ", "paragraph": "8. A method for producing transition metal composite hydroxide particles serving as a precursor of a positive electrode active material for a nonaqueous electrolyte secondary battery by a crystallization reaction, the method comprising:\na nucleus-forming step of controlling an aqueous solution for nucleus formation containing at least a transition metal-containing metal compound and an ammonium ion donor so that the aqueous solution for nucleus formation has a pH of 12.0 to 14.0 at a liquid temperature of 25 \u2103 and forming nuclei,\na particle growth step of controlling the aqueous solution for particle growth containing the nuclei obtained in the nucleus production step so that the pH of the aqueous solution for particle growth becomes lower than that in the nucleus production step at a liquid temperature of 25 \u2103 and 10.5 to 12.0 to grow the nuclei,\nand the reaction environment at the initial stage of the nucleus generation step and the particle growth step is a non-oxidizing environment having an oxygen concentration of 5% by volume or less,\nin the particle growth step, an environmental control is performed once in a range of 5% to 35% of the total time of the particle growth step from the start of the particle growth step, the environmental control being: the reaction environment is switched from the non-oxidizing environment to an oxidizing environment having an oxygen concentration of more than 5% by volume, and then from the oxidizing environment to a non-oxidizing environment having an oxygen concentration of 5% by volume or less, so that the crystallization reaction time in the oxidizing environment is 3% to 20% of the total time of the particle growth step.", "measurement_extractions": [ { "docId": "CN105122517B_8", "quantity": "12.0 to 14.0", "unit": null, "measured_entity": "aqueous solution for nucleus formation", "measured_property": "pH" }, { "docId": "CN105122517B_8", "quantity": "25 \u2103", "unit": "\u2103", "measured_entity": "aqueous solution for nucleus formation", "measured_property": "liquid temperature" }, { "docId": "CN105122517B_8", "quantity": "25 \u2103", "unit": null, "measured_entity": "the aqueous solution for particle growth", "measured_property": "liquid temperature" }, { "docId": "CN105122517B_8", "quantity": "10.5 to 12.0", "unit": null, "measured_entity": "the aqueous solution for particle growth", "measured_property": "pH" } ], "split": "train", "docId": "CN105122517B_8", "dataset": "bm" }, { "instruction": "\n You are an expert at extracting quantity, units and their related context from text. \n Given a paragraph below identify each quantity and its related unit and related context, i.e. the measured entity and measured property if they exist.\n ", "paragraph": "1. A method for producing a transition metal composite oxide, comprising: a 1 st step of preparing a 1 st internal formation metal salt aqueous solution and a 2 nd internal formation metal salt aqueous solution containing nickel, cobalt, and manganese and having different concentrations of the nickel, cobalt, and manganese from each other; step 2, supplying a chelating agent and an aqueous alkali solution into the reactor; a 3 rd step of continuously supplying and mixing the 1 st interior-forming metal salt aqueous solution, the chelating agent, and the alkali aqueous solution to the reactor, and culturing particles having a fixed concentration of nickel, cobalt, and manganese and containing the 1 st interior having a radius of r1(0.2 um. ltoreq. r 1. ltoreq.5 um); and a 4 th step of mixing and supplying the 1 st inside forming metal salt aqueous solution and the 2 nd inside forming metal salt aqueous solution in a mixing ratio gradually changing from 100 v%: 0 v% to 0 v%: 100 v%, while mixing the chelating agent and the alkali aqueous solution into the reactor, to form particles containing the 2 nd inside having a radius r2(r2 \u2266 10um) in the 1 st inside profile, characterized in that,\nthe concentration of the alkaline aqueous solution added in the reactor in the 2 nd step is adjusted according to the nickel concentration of the particles produced in the 3 rd step before the 3 rd step, and the concentration of the alkaline aqueous solution of the reaction solution in the 2 nd step is adjusted to 0.25g/L to 0.5g/L so that the pH of the solution in the reactor in the 2 nd step is adjusted to 11.8 to 12.3.", "measurement_extractions": [ { "docId": "CN105594029B_1", "quantity": "adjusted to 0.25g/L to 0.5g/L", "unit": "g/L", "measured_entity": "3 rd step", "measured_property": "the concentration of the alkaline aqueous solution" }, { "docId": "CN105594029B_1", "quantity": "to 11.8 to 12.3", "unit": null, "measured_entity": "the solution in the reactor", "measured_property": "pH" } ], "split": "train", "docId": "CN105594029B_1", "dataset": "bm" }, { "instruction": "\n You are an expert at extracting quantity, units and their related context from text. \n Given a paragraph below identify each quantity and its related unit and related context, i.e. the measured entity and measured property if they exist.\n ", "paragraph": "3. The method for producing a transferred-metal composite oxide according to claim 1,\nin the steps 1 to 4, the aqueous solution of the metal salt for forming the inside of the 1 st compartment, the chelating agent, and the aqueous alkali solution are mixed in the reactor so that the particle size distribution of the particles formed after the reaction for 30 minutes has D50 of 4um or less.", "measurement_extractions": [ { "docId": "CN105594029B_3", "quantity": "4um", "unit": "um", "measured_entity": "the particles", "measured_property": "D50" } ], "split": "train", "docId": "CN105594029B_3", "dataset": "bm" }, { "instruction": "\n You are an expert at extracting quantity, units and their related context from text. \n Given a paragraph below identify each quantity and its related unit and related context, i.e. the measured entity and measured property if they exist.\n ", "paragraph": "4. The method for producing a transferred-metal composite oxide according to claim 1,\nfurther comprising the step 5: drying or heat-treating the transition metal composite oxide obtained by performing the 1 st to 4 th steps,\nand the average diameter of the transfer metal composite oxide particles produced in the 5 th step is 5 to 10 um.", "measurement_extractions": [ { "docId": "CN105594029B_4", "quantity": "5 to 10 um", "unit": "um", "measured_entity": "transfer metal composite oxide particles", "measured_property": "average diameter" } ], "split": "train", "docId": "CN105594029B_4", "dataset": "bm" }, { "instruction": "\n You are an expert at extracting quantity, units and their related context from text. \n Given a paragraph below identify each quantity and its related unit and related context, i.e. the measured entity and measured property if they exist.\n ", "paragraph": "9. A method for producing a transition metal composite oxide,\nthe method comprises the following steps:\nmanufacturing a 1 st metal salt aqueous solution containing nickel, manganese and cobalt;\nmanufacturing an aqueous solution of a 2 nd metal salt containing nickel, manganese and cobalt;\nmixing an alkaline aqueous solution and an aqueous ammonia solution in a reactor, adjusting the concentration of the alkaline aqueous solution according to the nickel concentration of the 1 st metal salt aqueous solution, and adjusting the pH value in the reaction solution to 11.8 to 12.3; and\nsupplying a 1 st mixed metal salt aqueous solution mixing the 1 st metal salt aqueous solution and the 2 nd metal salt aqueous solution, ammonia, and an alkaline aqueous solution into the reactor,\nand a mixing ratio of the 1 st metal salt aqueous solution and the 2 nd metal salt aqueous solution in the 1 st mixed metal salt aqueous solution is 0 v% or more and 100 v% or less.", "measurement_extractions": [ { "docId": "CN105594029B_9", "quantity": "11.8 to 12.3", "unit": null, "measured_entity": "in the reaction solution", "measured_property": "pH" } ], "split": "train", "docId": "CN105594029B_9", "dataset": "bm" }, { "instruction": "\n You are an expert at extracting quantity, units and their related context from text. \n Given a paragraph below identify each quantity and its related unit and related context, i.e. the measured entity and measured property if they exist.\n ", "paragraph": "3. A positive electrode active material for a lithium secondary battery according to claim 1 or 2, characterized in, lithium transition metal composite oxide has a particle size distribution of not more than a maximum value of 2.", "measurement_extractions": [ { "docId": "CN105594031A_3", "quantity": "not more than a maximum value of 2", "unit": null, "measured_entity": "lithium transition metal composite oxide", "measured_property": "particle size distribution" } ], "split": "train", "docId": "CN105594031A_3", "dataset": "bm" }, { "instruction": "\n You are an expert at extracting quantity, units and their related context from text. \n Given a paragraph below identify each quantity and its related unit and related context, i.e. the measured entity and measured property if they exist.\n ", "paragraph": "5. The positive electrode for lithium secondary battery active material according to claim 4 in which a manufacturing method, characterized in, of a tap density of 1.4 g/cc or more precursors.", "measurement_extractions": [ { "docId": "CN105594031A_5", "quantity": "1.4 g/cc", "unit": "g/cc", "measured_entity": "precursors", "measured_property": "tap density" } ], "split": "train", "docId": "CN105594031A_5", "dataset": "bm" }, { "instruction": "\n You are an expert at extracting quantity, units and their related context from text. \n Given a paragraph below identify each quantity and its related unit and related context, i.e. the measured entity and measured property if they exist.\n ", "paragraph": "12. For a rechargeable battery positive electrode material of lithium metal oxide powder, having the general formula Li1+a M1-a O2, wherein M=Nix Mny Coz Av, Aas a dopant, wherein<0.30,0.55 \u2264 y \u2264 0.80 0.10 \u2264 a \u2264 0.25,0.10 \u2264 x, and the 02 /grepresented, also include sodium and sulfur impurities powder, wherein sodium % by weight represented by (Naweight) and sulfur (Sweight) sum of the contents (2 * Naweight) +Sweight exceeds 0.4 wt % and less than 1.6% by weight, and wherein the molar ratio of sodium to sulfur (Na/S) was 0.41+a M1-a O2, wherein M=Nix Mny Coz Av, Aas a dopant, wherein-0.05 \u2264 a \u2264 0.25,0.20 \u2264 x \u2264 0.90,0.10 \u2264 y \u2264 0.67, and a 0.10 \u2264 z \u2264 0.40, v \u2264 0.05, and the x + y + z + v=1, powder having a particle size distribution 10\u03bcm \u2264 D50 \u2264 20 \u00b5m, 0.9 \u2264 BET \u2264 5 has a specific surface, with BET m2 /grepresented, sodium and sulfur powder also includes impurities, wherein % by weight sodium expressed by (Naweight) and sulfur (Sweight) sum of the contents (2 * Naweight) +Sweight more than 0.4% and less than 1.6% by weight of the weight, and wherein the molar ratio of sodium to sulfur (Na/S) was 0.4Weight (D)) And sulfur (S)Weight (D)) Sum of contents (2. multidot. Na)Weight (D))+SWeight (D)More than 0.4 wt% and less than 1.6 wt%.", "measurement_extractions": [ { "docId": "CN106795008B_1", "quantity": "0.4 wt% and less than 1.6 wt%", "unit": "wt%", "measured_entity": "the precursor", "measured_property": "Sum of contents (2. multidot. Na)Weight (D))+SWeight (D)" } ], "split": "train", "docId": "CN106795008B_1", "dataset": "bm" }, { "instruction": "\n You are an expert at extracting quantity, units and their related context from text. \n Given a paragraph below identify each quantity and its related unit and related context, i.e. the measured entity and measured property if they exist.\n ", "paragraph": "11. A lithium metal oxide powder for use in a positive electrode material in a rechargeable battery having the general formula Li1+aM1-aO2Wherein M is NixMnyCozAvA is a dopant, wherein a is more than or equal to 0.10 and less than or equal to 0.25, and x is more than or equal to 0.10 and less than or equal to 0.252Expressed in terms of/g, said powder further comprising sodium and sulphur impurities, wherein said sodium (Na) is expressed in weight%Weight (D)) And sulfur (S)Weight (D)) Sum of contents (2. multidot. Na)Weight (D))+SWeight (D)More than 0.4% by weightAnd less than 1.6 wt%, and wherein the molar ratio of sodium to sulfur (Na/S) is 0.42Expressed in terms of/g, said powder further comprising sodium and sulphur impurities, wherein said sodium (Na) is expressed in weight%Weight (D)) And sulfur (S)Weight (D)) ComprisesSum of the amounts (2 Na)Weight (D))+SWeight (D)More than 0.4 wt% and less than 1.6 wt%, and wherein the molar ratio of sodium to sulfur (Na/S) is 0.41+aM1-aO2 where M= NixMnyCozAv, A being a dopant, wherein 0.10\u2264a\u22640.25, 0.10\u2264x\u22640.30, 0.55\u2264y\u22640.80, and 02/g, the powder further comprising a sodium and sulfur impurity, wherein the sum (2* Nawt)+ Swt of the sodium (Nawt) and sulfur (Swt) content expressed in wt% is more than 0.4 wt% and less than 1.6 wt%, and wherein the sodium to sulfur molar ratio (Na/S) is 0.42/g", "unit": "m2/g", "measured_entity": "lithium metal oxide powder", "measured_property": "specific surface area" }, { "docId": "EP3204973B1_10", "quantity": "is more than 0.4 wt% and less than 1.6 wt%", "unit": "wt%", "measured_entity": "sodium and sulfur", "measured_property": "the sodium (Nawt) and sulfur (Swt) content" } ], "split": "train", "docId": "EP3204973B1_10", "dataset": "bm" }, { "instruction": "\n You are an expert at extracting quantity, units and their related context from text. \n Given a paragraph below identify each quantity and its related unit and related context, i.e. the measured entity and measured property if they exist.\n ", "paragraph": "11. A method for preparing a carbonate precursor compound according to claim 2 or 3, the precursor compound having a sodium to sulfur molar ratio (Na/S) of 0.4wt)+ Swt of the sodium (Nawt) and sulfur (Swt) content expressed in wt% of more than 0.4 wt% and less than 1.6 wt%, comprising the steps of:\n- providing a feed solution comprising Ni-, Mn- and Co-ions, and a source of A, wherein the Ni-, Mn-, Co- and A-ions are present in a water soluble sulfate compound,\n- providing an ionic solution comprising a carbonate solution and Na-ions, wherein the CO3/SO4ratio is selected so as to obtain the Na/S molar ratio of the precursor compound,\n- providing a slurry comprising seeds comprising M'-ions, wherein M' = Nix'Mny'Coz'A'n',\nA' being a dopant, with 0\u2264x'\u22641, 0\u2264y'\u22641, 0\u2264z'\u22641, 0\u2264n'\u22641 and x'+y'+z'+n'=1,\n- mixing the feed solution, the ionic solution and the slurry in a reactor, thereby obtaining a reactive liquid mixture,\n- precipitating a carbonate onto the seeds in the reactive liquid mixture, thereby obtaining a reacted liquid mixture and the carbonate precursor, and\n- separating the carbonate precursor from the reacted liquid mixture.", "measurement_extractions": [ { "docId": "EP3204973B1_11", "quantity": "more than 0.4 wt% and less than 1.6 wt%", "unit": "wt%", "measured_entity": "sodium (Nawt) and sulfur", "measured_property": "content" } ], "split": "train", "docId": "EP3204973B1_11", "dataset": "bm" }, { "instruction": "\n You are an expert at extracting quantity, units and their related context from text. \n Given a paragraph below identify each quantity and its related unit and related context, i.e. the measured entity and measured property if they exist.\n ", "paragraph": "13. The method according to claim 11 or 12, wherein the concentration of NH3in the reactor is less than 5.0 g/L.", "measurement_extractions": [ { "docId": "EP3204973B1_13", "quantity": "less than 5.0 g/L", "unit": "g/L", "measured_entity": "NH3", "measured_property": "concentration" } ], "split": "train", "docId": "EP3204973B1_13", "dataset": "bm" }, { "instruction": "\n You are an expert at extracting quantity, units and their related context from text. \n Given a paragraph below identify each quantity and its related unit and related context, i.e. the measured entity and measured property if they exist.\n ", "paragraph": "16. The method according to any one of claims 11 to 15, wherein the seeds have a median particle size D50 between 0.1 and 3 \u00b5m.", "measurement_extractions": [ { "docId": "EP3204973B1_16", "quantity": "between 0.1 and 3 \u00b5m", "unit": "\u00b5m", "measured_entity": "the seeds", "measured_property": "median particle size D50" } ], "split": "train", "docId": "EP3204973B1_16", "dataset": "bm" }, { "instruction": "\n You are an expert at extracting quantity, units and their related context from text. \n Given a paragraph below identify each quantity and its related unit and related context, i.e. the measured entity and measured property if they exist.\n ", "paragraph": "6. A lithium metal oxide powder for a positive electrode material in a rechargeable battery, having the general formula Li1+aM1-aO2 where M= NixMnyCozAv, A being a dopant, wherein -0.05\u2264a\u22640.25, 0.20\u2264x\u22640.90, 0.10\u2264y\u22640.67, and 0.10\u2264z\u22640.40, v\u22640.05, and x+y+z+v=1, the powder having a particle size distribution with 10\u00b5m\u2264D50\u226420\u00b5m), a specific surface area with 0.9\u2264BET\u22645, the BET being expressed in m2/g, the powder further comprising a sodium and sulfur impurity, wherein the sum (2* Nawt)+ Swt of the sodium (Nawt) and sulfur (Swt) content expressed in wt% is more than 0.4 wt% and less than 1.6 wt%, and wherein the sodium to sulfur molar ratio (Na/S) is 0.42/g", "unit": "m2/g", "measured_entity": "lithium metal oxide powder", "measured_property": "specific surface area" }, { "docId": "EP3204973B1_6", "quantity": "is more than 0.4 wt% and less than 1.6 wt%", "unit": "wt%", "measured_entity": "lithium metal oxide powder", "measured_property": "sodium (Nawt) and sulfur (Swt) content" } ], "split": "train", "docId": "EP3204973B1_6", "dataset": "bm" }, { "instruction": "\n You are an expert at extracting quantity, units and their related context from text. \n Given a paragraph below identify each quantity and its related unit and related context, i.e. the measured entity and measured property if they exist.\n ", "paragraph": "5. The precursor of a positive electrode active material for a secondary battery of Claim 1, which has an average particle diameter (D50) of 7 \u00b5m to 20 \u00b5m and a BET specific surface area of 5.0 m2/g to 30.0 m2/g.", "measurement_extractions": [ { "docId": "EP3425706A1_5", "quantity": "7 \u00b5m to 20 \u00b5m", "unit": "\u00b5m", "measured_entity": "The precursor", "measured_property": "average particle diameter (D50" }, { "docId": "EP3425706A1_5", "quantity": "5.0 m2/g to 30.0 m2/g", "unit": "m2/g", "measured_entity": "The precursor", "measured_property": "BET specific surface area" } ], "split": "train", "docId": "EP3425706A1_5", "dataset": "bm" }, { "instruction": "\n You are an expert at extracting quantity, units and their related context from text. \n Given a paragraph below identify each quantity and its related unit and related context, i.e. the measured entity and measured property if they exist.\n ", "paragraph": "6. A method for preparing the precursor of a positive electrode active material for a secondary battery of Claim 1, the method comprising:\npreparing a metal-containing solution by mixing a nickel raw material, a cobalt raw material and a manganese raw material; and\nand introducing an ammonium cation-containing complex forming agent and a basic compound to the metal-containing solution and co-precipitation reacting the result under a pH of 10.50 to 12.00 and a temperature of 50\u00b0C to 70\u00b0C,\nwherein the ammonium cation-containing complex forming agent is introduced at a rate of 0.5 times to 1.5 times with respect to an introduction rate of the metal-containing solution.", "measurement_extractions": [ { "docId": "EP3425706A1_6", "quantity": "10.50 to 12.00", "unit": null, "measured_entity": "co-precipitation reacting", "measured_property": "pH" }, { "docId": "EP3425706A1_6", "quantity": "50\u00b0C to 70\u00b0C", "unit": "\u00b0C", "measured_entity": "co-precipitation reacting", "measured_property": "temperature" } ], "split": "train", "docId": "EP3425706A1_6", "dataset": "bm" }, { "instruction": "\n You are an expert at extracting quantity, units and their related context from text. \n Given a paragraph below identify each quantity and its related unit and related context, i.e. the measured entity and measured property if they exist.\n ", "paragraph": "9. The positive electrode active material for a secondary battery of Claim 8, which has an average particle diameter of 7 \u00b5m to 15 \u00b5m and a BET specific surface area of 0.1 m2/g to 1.0 m2/g.", "measurement_extractions": [ { "docId": "EP3425706A1_9", "quantity": "7 \u00b5m to 15 \u00b5m", "unit": "\u00b5m", "measured_entity": "positive electrode active material", "measured_property": "average particle diameter" }, { "docId": "EP3425706A1_9", "quantity": "0.1 m2/g to 1.0 m2/g", "unit": "m2/g", "measured_entity": "positive electrode active material", "measured_property": "BET specific surface area" } ], "split": "train", "docId": "EP3425706A1_9", "dataset": "bm" }, { "instruction": "\n You are an expert at extracting quantity, units and their related context from text. \n Given a paragraph below identify each quantity and its related unit and related context, i.e. the measured entity and measured property if they exist.\n ", "paragraph": "1. A nickel-based active material precursor for a lithium secondary battery, comprising:\na porous core; and\na shell having a radially arranged structure with a higher density than the porous core,\nwherein the nickel-based active material precursor has a size of about 9 \u00b5m to about 14 \u00b5m, and\nthe porous core has a volume of about 5 % by volume to about 20 % by volume based on the total volume of the nickel-based active material precursor.", "measurement_extractions": [ { "docId": "EP3550642A1_1", "quantity": "9 \u00b5m to about 14 \u00b5m", "unit": "\u00b5m", "measured_entity": "active material precursor", "measured_property": "size" } ], "split": "train", "docId": "EP3550642A1_1", "dataset": "bm" }, { "instruction": "\n You are an expert at extracting quantity, units and their related context from text. \n Given a paragraph below identify each quantity and its related unit and related context, i.e. the measured entity and measured property if they exist.\n ", "paragraph": "1. A process for preparing a nickel composite hydroxide with a mean particle diameter in the range from 3 to 20 \u00b5m (d50) comprising the step(s) of combining\n(a) an aqueous solution of water-soluble salts of nickel and of at least one of cobalt and manganese, and, optionally, at least one of Al, Mg, B, or transition metals other than nickel, cobalt, and manganese,\n(b) with an aqueous solution of an alkali metal hydroxide and\n(c) with an organic acid or alkali or ammonium salt of an organic acid or an anhydride of an organic acid whose nickel(+II) salt has a solubility of 1g/l or less in water at 20\u00b0C, and, optionally, with\n(d) an aqueous solution of alkali metal aluminate.", "measurement_extractions": [ { "docId": "EP3659974A1_1", "quantity": "in the range from 3 to 20 \u00b5m", "unit": "\u00b5m", "measured_entity": "A process for preparing", "measured_property": "particle diameter" } ], "split": "train", "docId": "EP3659974A1_1", "dataset": "bm" }, { "instruction": "\n You are an expert at extracting quantity, units and their related context from text. \n Given a paragraph below identify each quantity and its related unit and related context, i.e. the measured entity and measured property if they exist.\n ", "paragraph": "10. A nickel composite hydroxide in particulate form with a mean particle diameter in the range from 3 to 20 \u00b5m (d50), containing in the range of from 60 to 95 mole-% Ni and at least one transition metal selected from Co and Mn, and in the range of from 0.1 to 3.0 % by weight of carboxylate whose Ni(+II) salt has a solubility in water at 20\u00b0C of 1g/l or less, and the percentage referring to said nickel composite hydroxide.", "measurement_extractions": [ { "docId": "EP3659974A1_10", "quantity": "in the range from 3 to 20 \u00b5m", "unit": "\u00b5m", "measured_entity": "composite hydroxide", "measured_property": "particle diameter" } ], "split": "train", "docId": "EP3659974A1_10", "dataset": "bm" }, { "instruction": "\n You are an expert at extracting quantity, units and their related context from text. \n Given a paragraph below identify each quantity and its related unit and related context, i.e. the measured entity and measured property if they exist.\n ", "paragraph": "13. Nickel composite hydroxide according to any of claims 10 to 12 wherein said nickel composite hydroxide has a specific surface (BET) in the range of from 2 to 70 m2/g, determined according to.", "measurement_extractions": [ { "docId": "EP3659974A1_13", "quantity": "in the range of from 2 to 70 m2/g", "unit": "m2/g", "measured_entity": "composite hydroxide", "measured_property": "specific surface (BET" } ], "split": "train", "docId": "EP3659974A1_13", "dataset": "bm" }, { "instruction": "\n You are an expert at extracting quantity, units and their related context from text. \n Given a paragraph below identify each quantity and its related unit and related context, i.e. the measured entity and measured property if they exist.\n ", "paragraph": "14. Nickel composite hydroxide according to any of claims 10 to 13 wherein said nickel composite hydroxide has a width of particle diameter distribution, calculated as [(d90-d10)/(d50)] of at least 0.5.", "measurement_extractions": [ { "docId": "EP3659974A1_14", "quantity": "at least 0.5", "unit": null, "measured_entity": "composite hydroxide", "measured_property": "particle diameter distribution" } ], "split": "train", "docId": "EP3659974A1_14", "dataset": "bm" }, { "instruction": "\n You are an expert at extracting quantity, units and their related context from text. \n Given a paragraph below identify each quantity and its related unit and related context, i.e. the measured entity and measured property if they exist.\n ", "paragraph": "3. Process according to claim 1 or 2 wherein said process is carried out a pH value in the range of from 11 to 13.", "measurement_extractions": [ { "docId": "EP3659974A1_3", "quantity": "in the range of from 11 to 13", "unit": null, "measured_entity": "process", "measured_property": "pH value" } ], "split": "train", "docId": "EP3659974A1_3", "dataset": "bm" }, { "instruction": "\n You are an expert at extracting quantity, units and their related context from text. \n Given a paragraph below identify each quantity and its related unit and related context, i.e. the measured entity and measured property if they exist.\n ", "paragraph": "9. The method of claim 6, wherein the cobalt oxide particle and the manganese oxide particle each have an average particle diameter (D50) of 10-500 nm.", "measurement_extractions": [ { "docId": "EP3693340A2_9", "quantity": "10-500 nm", "unit": "nm", "measured_entity": "cobalt oxide particle and the manganese oxide particle", "measured_property": "average particle diameter (D50" } ], "split": "train", "docId": "EP3693340A2_9", "dataset": "bm" }, { "instruction": "\n You are an expert at extracting quantity, units and their related context from text. \n Given a paragraph below identify each quantity and its related unit and related context, i.e. the measured entity and measured property if they exist.\n ", "paragraph": "2. A method of manufacturing a positive electrode active material precursor for a non-aqueous electrolyte secondary battery, the method comprising:\na crystallization process performed in an atmosphere in which an oxygen concentration is less than or equal to 20 volume %, the crystallization process including crystallizing the positive electrode active material precursor including a nickel composite hydroxide particle, in a reaction solution including at least a mixed aqueous solution of a metal salt including nickel salt, an ammonium ion supplier, and an alkaline material, in which an ammonium ion concentration is greater than or equal to 5.0 g/L and a pH value is greater than or equal to 11.0 based on a liquid temperature of 50 \u00b0C.", "measurement_extractions": [ { "docId": "EP3719889A1_2", "quantity": "greater than or equal to 5.0 g/L", "unit": "g/L", "measured_entity": "active material precursor", "measured_property": "ammonium ion concentration" }, { "docId": "EP3719889A1_2", "quantity": "greater than or equal to 11.0", "unit": null, "measured_entity": "active material precursor", "measured_property": "pH value" } ], "split": "train", "docId": "EP3719889A1_2", "dataset": "bm" }, { "instruction": "\n You are an expert at extracting quantity, units and their related context from text. \n Given a paragraph below identify each quantity and its related unit and related context, i.e. the measured entity and measured property if they exist.\n ", "paragraph": "10. The positive electrode active material for a secondary battery of Claim 8, which has tap density of 1.7 g/cc to 3.0 g/cc.", "measurement_extractions": [ { "docId": "IN201817029065A_10", "quantity": "1.7 g/cc to 3.0 g/cc", "unit": "g/cc", "measured_entity": "positive electrode active material", "measured_property": "tap density" } ], "split": "train", "docId": "IN201817029065A_10", "dataset": "bm" }, { "instruction": "\n You are an expert at extracting quantity, units and their related context from text. \n Given a paragraph below identify each quantity and its related unit and related context, i.e. the measured entity and measured property if they exist.\n ", "paragraph": "5. The precursor of a positive electrode active material for a secondary battery of Claim 1, which has an average particle diameter (D50) of 7 .micro.m to 20 .micro.m and a BET specific surface area of 5.0 m2/g to 30.0 m2/g.", "measurement_extractions": [ { "docId": "IN201817029065A_5", "quantity": "7 .micro.m to 20 .micro.m", "unit": "micro.m", "measured_entity": "The precursor", "measured_property": "average particle diameter (D50" }, { "docId": "IN201817029065A_5", "quantity": "5.0 m2/g to 30.0 m2/g", "unit": "m2/g", "measured_entity": "The precursor", "measured_property": "BET specific surface area" } ], "split": "train", "docId": "IN201817029065A_5", "dataset": "bm" }, { "instruction": "\n You are an expert at extracting quantity, units and their related context from text. \n Given a paragraph below identify each quantity and its related unit and related context, i.e. the measured entity and measured property if they exist.\n ", "paragraph": "6. A method for preparing the precursor of a positive electrode active material for a secondary battery of Claim 1, the method comprising: preparing a metal-containing solution by mixing a nickel raw material, a cobalt raw material and a manganese raw material;\nand and introducing an ammonium cation-containing complex forming agent and a basic compound to the metal-containing solution and co-precipitation reacting the result under a pH of 10.50 to 12.00 and a temperature of 50C to 70C, wherein the ammonium cation-containing complex forming agent is introduced at a rate of 0.5 times to 1.5 times with respect to an introduction rate of the metalcontaining solution.", "measurement_extractions": [ { "docId": "IN201817029065A_6", "quantity": "10.50 to 12.00", "unit": null, "measured_entity": "pH", "measured_property": null }, { "docId": "IN201817029065A_6", "quantity": "50C to 70C", "unit": "C", "measured_entity": "temperature", "measured_property": null } ], "split": "train", "docId": "IN201817029065A_6", "dataset": "bm" }, { "instruction": "\n You are an expert at extracting quantity, units and their related context from text. \n Given a paragraph below identify each quantity and its related unit and related context, i.e. the measured entity and measured property if they exist.\n ", "paragraph": "9. The positive electrode active material for a secondary battery of Claim 8, which has an average particle diameter of 7 .micro.m to 15 .micro.m and a BET specific surface area of 0.1 m2/g to 1.0 m2/g.", "measurement_extractions": [ { "docId": "IN201817029065A_9", "quantity": "7 .micro.m to 15 .micro.m", "unit": "micro.m", "measured_entity": "positive electrode active material", "measured_property": "average particle diameter" }, { "docId": "IN201817029065A_9", "quantity": "0.1 m2/g to 1.0 m2/g", "unit": "m2/g", "measured_entity": "positive electrode active material", "measured_property": "BET specific surface area" } ], "split": "train", "docId": "IN201817029065A_9", "dataset": "bm" }, { "instruction": "\n You are an expert at extracting quantity, units and their related context from text. \n Given a paragraph below identify each quantity and its related unit and related context, i.e. the measured entity and measured property if they exist.\n ", "paragraph": "5. The method for producing the positive active material for a lithium secondary battery according to claim 4, wherein the precursor has a tap density of 1.4 g/cc or more.", "measurement_extractions": [ { "docId": "US10319998B2_5", "quantity": "1.4 g/cc", "unit": "g/cc", "measured_entity": "precursor", "measured_property": "tap density" } ], "split": "train", "docId": "US10319998B2_5", "dataset": "bm" }, { "instruction": "\n You are an expert at extracting quantity, units and their related context from text. \n Given a paragraph below identify each quantity and its related unit and related context, i.e. the measured entity and measured property if they exist.\n ", "paragraph": "The invention claimed is:\n1. A lithium metal oxide powder for a positive electrode material in a rechargeable battery, having the general formula Li1+aM1\u2212aO2 where M=NixMnyCozAv, A being a dopant, wherein \u22120.05\u2264a\u22640.25, 0.20\u2264x\u22640.90, 0.10\u2264y\u22640.67, and 0.10\u2264z\u22640.40, v\u22640.05, and x+y+z+v=1, the powder having a particle size distribution with 10 \u03bcm\u2264D50\u226420 \u03bcm, a specific surface with 0.9\u2264BET\u22645, the BET being expressed in m2/g, the powder further comprising a sodium and sulfur impurity, wherein the sum (2*Nawt)+Swt of the sodium (Nawt) and sulfur (Swt) content expressed in wt % is more than 0.4 wt % and less than 1.6 wt %, and wherein the sodium to sulfur molar ratio (Na/S) is 0.42/g", "unit": "m2/g", "measured_entity": "the powder", "measured_property": "specific surface" }, { "docId": "US10411258B2_1", "quantity": "more than 0.4 wt % and less than 1.6 wt %", "unit": "wt %", "measured_entity": "sodium and sulfur impurity", "measured_property": "(2*Nawt)+Swt of the sodium (Nawt) and sulfur (Swt)" } ], "split": "train", "docId": "US10411258B2_1", "dataset": "bm" }, { "instruction": "\n You are an expert at extracting quantity, units and their related context from text. \n Given a paragraph below identify each quantity and its related unit and related context, i.e. the measured entity and measured property if they exist.\n ", "paragraph": "What is claimed is:\n1. A precursor of a positive electrode active material for a secondary battery, comprising:\na secondary particle having a single layer structure, wherein the single layer structure is an aggregate of pillar-shaped primary particles radially oriented in a surface direction from the particle center of the secondary particle,\nwherein\nthe primary particle includes a composite metal hydroxide of Ni\u2014Co\u2014Mn of the following Chemical Formula 1:\nNi1\u2212(x+y+z)CoxMyMnz(OH)2[Chemical Formula 1]\nwherein, in Chemical Formula 1,\nM includes any one, or two or more elements selected from the group consisting of Al, Zr, Mg, Zn, Y, Fe and Ti; and\nx, y and z are each 0wt)+Swt of the sodium (Nawt) and sulfur (Swt) content" } ], "split": "train", "docId": "US20190386303A1_1", "dataset": "bm" }, { "instruction": "\n You are an expert at extracting quantity, units and their related context from text. \n Given a paragraph below identify each quantity and its related unit and related context, i.e. the measured entity and measured property if they exist.\n ", "paragraph": "1. A carbonate precursor compound for manufacturing a lithium metal (M)-oxide powder usable as an active positive electrode material in lithium-ion batteries, M comprising 20 to 90 mol % Ni, 10 to 70 mol % Mn and 10 to 40 mol % Co, the precursor further comprising a sodium and sulfur impurity, wherein the sodium to sulfur molar ratio (Na/S) is 0.4wt)+Swt of the sodium (Nawt) and sulfur (Swt) content expressed in wt % is more than 0.4 wt % and less than 1.6 wt %.", "measurement_extractions": [ { "docId": "US20190386303A1_11", "quantity": "less than 5.0 g/L", "unit": "g/L", "measured_entity": "NH3in the reactor", "measured_property": "concentration" } ], "split": "train", "docId": "US20190386303A1_11", "dataset": "bm" }, { "instruction": "\n You are an expert at extracting quantity, units and their related context from text. \n Given a paragraph below identify each quantity and its related unit and related context, i.e. the measured entity and measured property if they exist.\n ", "paragraph": "11. The method according to claim 7, wherein the concentration of NH3in the reactor is less than 5.0 g/L.", "measurement_extractions": [ { "docId": "US20190386303A1_14", "quantity": "between 0.1 and 3 \u03bcm", "unit": "\u03bcm", "measured_entity": "seeds", "measured_property": "median particle size D50" } ], "split": "train", "docId": "US20190386303A1_14", "dataset": "bm" }, { "instruction": "\n You are an expert at extracting quantity, units and their related context from text. \n Given a paragraph below identify each quantity and its related unit and related context, i.e. the measured entity and measured property if they exist.\n ", "paragraph": "14. The method according to claim 7, wherein the seeds have a median particle size D50 between 0.1 and 3 \u03bcm.", "measurement_extractions": [ { "docId": "US20190386303A1_15", "quantity": "0.4wt) and sulfur (Swt) content", "measured_property": null } ], "split": "train", "docId": "US20190386303A1_15", "dataset": "bm" }, { "instruction": "\n You are an expert at extracting quantity, units and their related context from text. \n Given a paragraph below identify each quantity and its related unit and related context, i.e. the measured entity and measured property if they exist.\n ", "paragraph": "15. A method for preparing the carbonate precursor compound of claim 2, comprising:\nproviding a feed solution comprising Ni-, Mn- and Co-ions, and a source of A, wherein the Ni-, Mn-, Co- and A-ions are present in a water soluble sulfate compound,\nproviding an ionic solution comprising a carbonate solution and Na-ions, wherein the CO3/SO4 rate is selected so as to obtain a Na/S molar ratio with 0.4wt) and sulfur (Swt) content expressed in wt % yield a sum (2*Nawt)+Swt of more than 0.4 wt % and less than 1.6 wt %,\nproviding a slurry comprising seeds comprising M\u2032-ions, wherein M\u2032=NixMnyCozA\u2032n,\nA\u2032 being a dopant, with 0\u2264x\u2032\u22641, 0\u2264y\u2032\u22641, 0\u2264z\u2032\u22641, 0\u2264n\u2032\u22641 and x\u2032+y\u2032+z\u2032+n\u2032=1,\nmixing the feed solution, the ionic solution and the slurry in the reactor, thereby obtaining a reactive liquid mixture,\nprecipitating a carbonate onto the seeds in the reactive liquid mixture, thereby obtaining a reacted liquid mixture and the carbonate precursor, and\nseparating the carbonate precursor from the reacted liquid mixture.", "measurement_extractions": [ { "docId": "US20190386303A1_5", "quantity": "is between 0.1 and 0.7 wt %", "unit": "wt %", "measured_entity": "carbonate precursor", "measured_property": "sodium content" }, { "docId": "US20190386303A1_5", "quantity": "is between 0.2 and 0.9 wt %", "unit": "wt %", "measured_entity": "carbonate precursor", "measured_property": "sulfur content" } ], "split": "train", "docId": "US20190386303A1_5", "dataset": "bm" }, { "instruction": "\n You are an expert at extracting quantity, units and their related context from text. \n Given a paragraph below identify each quantity and its related unit and related context, i.e. the measured entity and measured property if they exist.\n ", "paragraph": "5. The carbonate precursor compound of claim 1, wherein the sodium content is between 0.1 and 0.7 wt %, and the sulfur content is between 0.2 and 0.9 wt %.", "measurement_extractions": [ { "docId": "US20190386303A1_6", "quantity": "10 \u03bcm\u2264D50\u226420 \u03bcm", "unit": "\u03bcm", "measured_entity": "powder", "measured_property": "particle size distribution" }, { "docId": "US20190386303A1_6", "quantity": "0.9\u2264BET\u22645, the BET being expressed in m2/g", "unit": "m2/g", "measured_entity": "powder", "measured_property": "specific surface" }, { "docId": "US20190386303A1_6", "quantity": "is more than 0.4 wt % and less than 1.6 wt %", "unit": "wt %", "measured_entity": "sodium and sulfur impurity", "measured_property": "the sum (2*Nawt)+Swt of the sodium (Nawt) and sulfur (Swt) content" } ], "split": "train", "docId": "US20190386303A1_6", "dataset": "bm" }, { "instruction": "\n You are an expert at extracting quantity, units and their related context from text. \n Given a paragraph below identify each quantity and its related unit and related context, i.e. the measured entity and measured property if they exist.\n ", "paragraph": "6. A lithium metal oxide powder for a positive electrode material in a rechargeable battery, having the general formula Li1+aM1\u2212aO2 where M=NixMnyCozAv, A being a dopant, wherein 0.10\u2264a<0.25, 0.10\u2264x<0.30, 0.55\u2264y\u22640.80, and 02/g, the powder further comprising a sodium and sulfur impurity, wherein the sum (2*Nawt)+Swt of the sodium (Nawt) and sulfur (Swt) content expressed in wt % is more than 0.4 wt % and less than 1.6 wt %, and wherein the sodium to sulfur molar ratio (Na/S) is 0.4wt) and sulfur (Swt) content", "measured_property": null } ], "split": "train", "docId": "US20190386303A1_7", "dataset": "bm" }, { "instruction": "\n You are an expert at extracting quantity, units and their related context from text. \n Given a paragraph below identify each quantity and its related unit and related context, i.e. the measured entity and measured property if they exist.\n ", "paragraph": "7. A method for preparing a carbonate precursor compound according to claim 1, comprising:\nproviding a feed solution comprising Ni-, Mn- and Co-ions, and a source of A, wherein the Ni-, Mn-, Co- and A-ions are present in a water soluble sulfate compound,\nproviding an ionic solution comprising a carbonate solution and Na-ions, wherein the CO3/SO4 rate is selected so as to obtain a Na/S molar ratio with 0.4wt) and sulfur (Swt) content expressed in wt % yield a sum (2*Nawt)+Swt of more than 0.4 wt % and less than 1.6 wt %,\nproviding a slurry comprising seeds comprising M\u2032-ions, wherein M\u2032=NixMnyCozA\u2032n,\nA\u2032 being a dopant, with 0\u2264x\u2032\u22641, 0\u2264y\u2032\u22641, 0\u2264z\u2032\u22641, 0\u2264n\u2032\u22641 and x\u2032+y\u2032+z\u2032+n\u2032=1,\nmixing the feed solution, the ionic solution and the slurry in the reactor, thereby obtaining a reactive liquid mixture,\nprecipitating a carbonate onto the seeds in the reactive liquid mixture, thereby obtaining a reacted liquid mixture and the carbonate precursor, and\nseparating the carbonate precursor from the reacted liquid mixture.", "measurement_extractions": [ { "docId": "US20200006770A1_1", "quantity": "12.0 to 14.0", "unit": null, "measured_entity": "nucleation process", "measured_property": "pH" }, { "docId": "US20200006770A1_1", "quantity": "less than in the nucleation process and is 10.5 to 12.0", "unit": null, "measured_entity": "particle growth process", "measured_property": "pH" } ], "split": "train", "docId": "US20200006770A1_1", "dataset": "bm" }, { "instruction": "\n You are an expert at extracting quantity, units and their related context from text. \n Given a paragraph below identify each quantity and its related unit and related context, i.e. the measured entity and measured property if they exist.\n ", "paragraph": "What is claimed is:\n1. A production method for producing transition metal composite hydroxide particles by a crystallization reaction to be a precursor for a cathode active material for a non-aqueous electrolyte rechargeable battery, comprising:\na nucleation process for performing nucleation by controlling an aqueous solution for nucleation that includes a metal compound that includes at least a transition metal and an ammonium ion donor so that the pH value at a standard liquid temperature of 25\u00b0 C. becomes 12.0 to 14.0; and\na particle growth process for causing nuclei to grow by controlling an aqueous solution for particle growth that includes the nuclei that were obtained in the nucleation process so that the pH value is less than in the nucleation process and is 10.5 to 12.0;\nthe reaction atmosphere in the nucleation process and at the beginning of the particle growth process being a non-oxidizing atmosphere in which an oxygen concentration is 5% by volume or less; and\nin the particle growth process, atmosphere control by which the reaction atmosphere is switched from the non-oxidizing atmosphere to an oxidizing atmosphere in which the oxygen concentration is greater than 5% by volume at timing from the start of the particle growth process within a range of 5% to 35% of the overall particle growth process time, and is then switched from the oxidizing atmosphere to a non-oxidizing atmosphere in which the oxygen concentration is 5% by volume or less so that the crystallization time in the oxidizing atmosphere in the particle growth process is 3% to 20% of the overall particle growth process time being performed at least one time.", "measurement_extractions": [ { "docId": "US20200006770A1_2", "quantity": "12.0 to 14.0", "unit": null, "measured_entity": "nucleation process", "measured_property": "pH" }, { "docId": "US20200006770A1_2", "quantity": "less than in the nucleation process and is 10.5 to 12.0", "unit": null, "measured_entity": "particle growth process", "measured_property": "pH" } ], "split": "train", "docId": "US20200006770A1_2", "dataset": "bm" }, { "instruction": "\n You are an expert at extracting quantity, units and their related context from text. \n Given a paragraph below identify each quantity and its related unit and related context, i.e. the measured entity and measured property if they exist.\n ", "paragraph": "2. A production method for producing transition metal composite hydroxide particles by a crystallization reaction to be a precursor for a cathode active material for a non-aqueous electrolyte rechargeable battery, comprising:\na nucleation process for performing nucleation by controlling an aqueous solution for nucleation that includes a metal compound that includes at least a transition metal and an ammonium ion donor so that the pH value at a standard liquid temperature of 25\u00b0 C. becomes 12.0 to 14.0; and\na particle growth process for causing nuclei to grow by controlling an aqueous solution for particle growth that includes the nuclei that were obtained in the nucleation process so that the pH value is less than in the nucleation process and is 10.5 to 12.0;\nthe reaction atmosphere in the nucleation process and at the beginning of the particle growth process being a non-oxidizing atmosphere in which the oxygen concentration is 5% by volume or less;\nin the particle growth process, atmosphere control by which the reaction atmosphere is switched from the non-oxidizing atmosphere to an oxidizing atmosphere in which the oxygen concentration is greater than 5% by volume, and is then switched from that oxidizing atmosphere to a non-oxidizing atmosphere in which the oxygen concentration is 5% by volume or less being performed two times or more; and\nthe total crystallization reaction time in the oxidizing atmosphere in the particle growth process being 3% to 30% of the total particle growth process time, and the crystallization reaction time during each oxidizing atmosphere being 1% or more of the total particle growth process time.", "measurement_extractions": [ { "docId": "US20200006770A1_6", "quantity": "1 \u03bcm to 15 \u03bcm", "unit": "\u03bcm", "measured_entity": "the secondary particles", "measured_property": "average particle size" }, { "docId": "US20200006770A1_6", "quantity": "0.65 or less", "unit": null, "measured_entity": "the secondary particles", "measured_property": "particle size distribution" } ], "split": "train", "docId": "US20200006770A1_6", "dataset": "bm" }, { "instruction": "\n You are an expert at extracting quantity, units and their related context from text. \n Given a paragraph below identify each quantity and its related unit and related context, i.e. the measured entity and measured property if they exist.\n ", "paragraph": "6. Transition metal composite hydroxide particles that are the precursor for cathode active material for a non-aqueous electrolyte rechargeable battery, comprising secondary particles that are formed by an aggregation of plate-shaped primary particles and fine primary particles that are smaller than the plate-shaped primary particles;\nthe secondary particles having a center section that is formed by an aggregation of the plate-shaped primary particles, and one layered structure of a low-density section that is formed by an aggregation of the fine primary particles and a high-density section that is formed by an aggregation of the plate-shaped primary particles on the outside of the center section;\nthe average value of the ratio of the center section outer diameter with respect to the particle size of the secondary particles being 30% to 80%, and the average value of the high-density section radial direction thickness with respect to the particle size of the secondary particles being 5% to 25%; and\nthe secondary particles having an average particle size of 1 \u03bcm to 15 \u03bcm, and an index [(d90\u2212d10)/average particle size] that indicates the extent of the particle size distribution of 0.65 or less.", "measurement_extractions": [ { "docId": "US20200006770A1_7", "quantity": "1 \u03bcm to 15 \u03bcm", "unit": "\u03bcm", "measured_entity": "the secondary particles", "measured_property": "average particle size" }, { "docId": "US20200006770A1_7", "quantity": "0.65 or less", "unit": null, "measured_entity": "the secondary particles", "measured_property": "particle size distribution" } ], "split": "train", "docId": "US20200006770A1_7", "dataset": "bm" }, { "instruction": "\n You are an expert at extracting quantity, units and their related context from text. \n Given a paragraph below identify each quantity and its related unit and related context, i.e. the measured entity and measured property if they exist.\n ", "paragraph": "7. Transition metal composite hydroxide particles that are the precursor for cathode active material for a non-aqueous electrolyte rechargeable battery, comprising secondary particles that are formed by an aggregation of plate-shaped primary particles and fine primary particles that are smaller than the plate-shaped primary particles;\nthe secondary particles having a center section that is formed by an aggregation of plate-shaped primary particles, and two or more layered structure of a low-density section that is formed by an aggregation of the fine primary particles and a high-density section that is formed by an aggregation of the plate-shaped primary particles on the outside of the center section; and\nthe secondary particles having an average particle size of 1 \u03bcm to 15 \u03bcm, and an index [(d90\u2212d10)/average particle size] that indicates the extent of the particle size distribution of 0.65 or less.", "measurement_extractions": [ { "docId": "US20200313194A1_4", "quantity": "a range of 5 \u03bcm to 10 \u03bcm", "unit": "\u03bcm", "measured_entity": "the transition metal precursor", "measured_property": "average particle diameter (D50" }, { "docId": "US20200313194A1_4", "quantity": "in the range of 400\u00b0 C. to 600\u00b0 C", "unit": "\u00b0 C", "measured_entity": "the first temperature holding section", "measured_property": "temperature" } ], "split": "train", "docId": "US20200313194A1_4", "dataset": "bm" }, { "instruction": "\n You are an expert at extracting quantity, units and their related context from text. \n Given a paragraph below identify each quantity and its related unit and related context, i.e. the measured entity and measured property if they exist.\n ", "paragraph": "4. The method of claim 1, wherein, when an average particle diameter (D50) of the transition metal precursor is in a range of 5 \u03bcm to 10 \u03bcm, the temperature of the first temperature holding section is in the range of 400\u00b0 C. to 600\u00b0 C.", "measurement_extractions": [ { "docId": "US20200313194A1_5", "quantity": "greater than 10 \u03bcm", "unit": "\u03bcm", "measured_entity": "the transition metal precursor", "measured_property": "average particle diameter (D50" }, { "docId": "US20200313194A1_5", "quantity": "in the range of 500\u00b0 C. to 650\u00b0 C", "unit": "\u00b0 C", "measured_entity": "the first temperature holding section", "measured_property": "temperature" } ], "split": "train", "docId": "US20200313194A1_5", "dataset": "bm" }, { "instruction": "\n You are an expert at extracting quantity, units and their related context from text. \n Given a paragraph below identify each quantity and its related unit and related context, i.e. the measured entity and measured property if they exist.\n ", "paragraph": "5. The method of claim 1, wherein an average particle diameter (D50) of the transition metal precursor is greater than 10 \u03bcm, the temperature of the first temperature holding section is in the range of 500\u00b0 C. to 650\u00b0 C.", "measurement_extractions": [ { "docId": "WO2008043558A1_12", "quantity": "less than 1.4", "unit": null, "measured_entity": "Pulverulent compound", "measured_property": "particle size distribution" } ], "split": "train", "docId": "WO2008043558A1_12", "dataset": "bm" }, { "instruction": "\n You are an expert at extracting quantity, units and their related context from text. \n Given a paragraph below identify each quantity and its related unit and related context, i.e. the measured entity and measured property if they exist.\n ", "paragraph": "12. Pulverulent compound according to at least one of Claims 1 to 11, characterized in that the normalized width of the particle size distribution, measured according to the Formula (1) D90 -DlO D50 in which D denotes the diameter of the secondary particles, is less than 1.4.", "measurement_extractions": [ { "docId": "WO2008043558A1_13", "quantity": "less than 1.2", "unit": null, "measured_entity": "Pulverulent compound", "measured_property": "particle size distribution" } ], "split": "train", "docId": "WO2008043558A1_13", "dataset": "bm" }, { "instruction": "\n You are an expert at extracting quantity, units and their related context from text. \n Given a paragraph below identify each quantity and its related unit and related context, i.e. the measured entity and measured property if they exist.\n ", "paragraph": "13. Pulverulent compound according to at least one of Claims 1 to 11, characterized in that the normalized width of the particle size distribution, measured according to the Formula (1) D90 -DlO 1) D50 in which D denotes the diameter of the secondary particles, is less than 1.2.", "measurement_extractions": [ { "docId": "WO2008043558A1_14", "quantity": "3.2 g/cm3", "unit": "g/cm3", "measured_entity": "Pulverulent compound", "measured_property": "compressed density" } ], "split": "train", "docId": "WO2008043558A1_14", "dataset": "bm" }, { "instruction": "\n You are an expert at extracting quantity, units and their related context from text. \n Given a paragraph below identify each quantity and its related unit and related context, i.e. the measured entity and measured property if they exist.\n ", "paragraph": "14. Pulverulent compound according to at least one of Claims 1 to 13, characterized in that it has a compressed density of at least 3.2 g/cm3at a compression pressure of 200 MPa.", "measurement_extractions": [ { "docId": "WO2008043558A1_15", "quantity": "at least 2.2 g/cm3", "unit": "g/cm3", "measured_entity": "Pulverulent compound", "measured_property": "tapped density" } ], "split": "train", "docId": "WO2008043558A1_15", "dataset": "bm" }, { "instruction": "\n You are an expert at extracting quantity, units and their related context from text. \n Given a paragraph below identify each quantity and its related unit and related context, i.e. the measured entity and measured property if they exist.\n ", "paragraph": "15. Pulverulent compound according to at least one of Claims 1 to 14, characterized in that it has a tapped density measured according to ASTM B 527, of at least 2.2 g/cm3.", "measurement_extractions": [ { "docId": "WO2008043558A1_16", "quantity": "at least 2.4 g/cm3", "unit": "g/cm3", "measured_entity": "Pulverulent compound", "measured_property": "tapped density" } ], "split": "train", "docId": "WO2008043558A1_16", "dataset": "bm" }, { "instruction": "\n You are an expert at extracting quantity, units and their related context from text. \n Given a paragraph below identify each quantity and its related unit and related context, i.e. the measured entity and measured property if they exist.\n ", "paragraph": "16. Pulverulent compound according to at least one of Claims 1 to 14, characterized in that it has a tapped density measured according to ASTM B 527, of at least 2.4 g/cm3.", "measurement_extractions": [ { "docId": "WO2020128714A1_3", "quantity": "equal to or greater than 3.7 g/cm3", "unit": "g/cm3", "measured_entity": "The cathode material", "measured_property": "pressed density" } ], "split": "train", "docId": "WO2020128714A1_3", "dataset": "bm" } ]